本人初学。在看一篇关于有无机杂化的论文,其中关于SAXS的图像实在是看不懂,求指点啊
- 图中横纵坐标分别代表什么?
- 图里的几个数值:33.2nm,36.2nm,2.94nm分别是什么意思呢?
相关原文:
The structural transitions of LC phases of hybrid L1/T1 were examined by small-angle X-ray scattering (SAXS) measurements.15
Figure 3 shows the SAXS profiles of hybrid L1/T1 and of a single component of L1. The scattering profiles of L1/T1 at 70, 90, and
110 °C (Figure 3a-c) suggested the existence of periodic particle interactions at an interval of 33.2 nm, corresponding to the total
width of a T1 particle covered with LC molecules. Therefore, the mesomorphic phase seems to have a nematic-like one-dimensional
order in the direction of the long axis of the acicular particles. Figure 3f shows a profile of the single component of L1 at 70 °C, in which
the sharp peak at 2.94 nm corresponds to the thickness of a layer unit of the smectic multilayer structure.
本人翻译:
L1/T1杂化的液晶相结构转变通过X射线小角散射测量法(SAXS)检测。15图3为L1/T1杂化和一个L1单组分的SAXS曲线。
L1/T1在70,90,和110°C的散射图像(图3a-c)说明了在33.2nm区间内周期性粒子相互作用的存在,
相应的T1粒子则覆盖了液晶分子的总宽度。因此,介晶相看上去在针状粒子长轴方向上有向列状的一维顺序。
图3f显示在70°C时单组分L1的轮廓,在2.94 nm处达到顶点,相应近晶型多层结构的一个层。
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